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GCMS surrogate recovery results for sample AE00310, Jan 2002

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Laboratory record documenting GCMS surrogate recovery data for sample AE00310 analyzed on January 10, 2002.

NYC-WTC_000050948–000050962

Folder label: “GCMS X 1/7/02 A 1/9/02

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Scanned page image, NYC-WTC_000050960
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NYC 9/11 Public Portal Document LLDL a y ‘r’X —

Data File : C: \MSDCHEM\1\5973N\02JAN09\310.D Vial: 8 Acq On : 10 Jan 2002 12:02 am Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.47 ug/L 399106 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 80 3 Phenanthrene-dlO 188 C14D10 001517-22-2 78 4 Cycloheptanone, 4 -phenyl- 188 C13H16O 067688-28-2 50 Abundance Scan 1699 (22.771 min): 310.0 (-) m/z 188.10 100.00% 188

5000

--------------- 80 22.40 22.60 22.80 23.00 23.20 43 57 66 94 108 118 132 146 158 0- —HH+ 1+4+—PmWITTTTTTTT m/z 189.15 18.00% /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 T 1 22.40 22.60 22.80 23.00 23.20 80 94 m/z80.10 14.83% 66 158 I I 01 TPPTTTHT i111H"1 m1 7 H44l r n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- US ........................ ........... .. 22.40 22.60 22.80 23.00 23.20 5000 m/z94.10 11.45% j — 80 94 160 , .

m/z-> 0- T TTTT ITTTT 40 50 mm 66 । । .. . ... t0 i''" i1'111" i 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 - 188 22 40 22.60 22.80 23.00 23.20 m/z 184.10 10.83%

5000

80 94 160 66 0 1 "T FTTIs - — J I ! I I J I-I I IT’Ti #!.... m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

310.D SCANS08.M Thu Jan 10 11:52:09 2002 Page 8

NYC-WTC_000050960

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NYC-WTC_000050960Source: NYC Law Department, mirrored locally

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