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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document —W fla.—C 1 wa—Citt ACPA

Data Pile : C: \MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 > Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrument Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rVB 36593 53144 0.36% 0.067% 2 4.241 71 76 83 rVB2 22960 50058 0.34% 0.063% 3 4.618 107 109 117 rBV3 17044 40548 0.28% 0.051% 4 4.835 123 128 141 rBV2 27934 79981 0.55% 0.101% 5 5.006 141 143 153 rVB 61576 108168 0.74% 0.137% 6 5.714 201 205 209 rBV 39086 70128 0.48% 0.089% 7 5.885 217 220 249 rVB 706749 1456863 9.95% 1.847% / 8 9.539 535 540 545 rW 37873 93991 0.64% 0.119% 9 9.630 545 548 551 rW 44739 101465 0.69% 0.129% 10 9.710 551 555 561 rW 4459840 9030017 61.70% 11.447% 11 9.836 561 566 587 rW 60998 216085 1.48% 0.274% 12 12.541 799 803 809 rW 24172 42117 0.29% 0.053% 13 13.192 855 860 865 rBV 6417484 12966032 88.60% 16.437% 14 18.341 1305 1311 1315 rBV 6948269 13858480 94.69% 17.568% 15 22.280 1651 1656 1661 rBV 56924 105083 0.72% 0.133% 16 22.645 1681 1688 1693 rBV 6503308 14635114 100.00% .18.552% 17 22.771 1695 1699 1713 rVB 89954 275151 1.88% 0.349% 18 27.726 2129 2133 2139 rBV 920554 1616302 11.04% 2.049% 19 30.500 2369 2376 2381 rBV 5446302 13095685 89.48% 16.601% 20 34.416 2713 2719 2763 rW 3935059 10990979 75.10% 13.933%

Sum of corrected areas: 78885391

30108.D SCAN508.M Mon Jan 28 09:49:58 2002 Page 1

NYC-WTC_000050758

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NYC-WTC_000050758Source: NYC Law Department, mirrored locally

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