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GCMS analysis results for sample AE00168, Jan 2002

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Laboratory report for sample AE00168 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050500–000050518

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN24\00168.D Vial: 1 Acq Ort : 24 Jan 2002 2:59 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.476 7 9 13 rVB 31653 43334 0.30% 0.057% 2 3.602 15 20 25 rBV 33853 48845 0.34% 0.064% 3 4.241 73 76 85 rVB5 9645 34250 0.24% 0.045% 4 4.618 107 109 115 rBV2 16331 40152 0.28% 0.053% 5 4.846 123 129 141 rBV4 25036 95892 0.66% 0.126% 6 5.006 141 143 149 rVB 23249 45260 0.31% 0.059% 7 5.885 217 220 227 rBV 776524 1597408 11.02% 2.093% 8 9.721 551 556 563 rW 4093382 8505727 58.70% 11.142% 9 12.541 799 803 809 rVB 13952 23493 0.16% 0.031% 10 13.192 855 860 865 rBV 6121921 12392333 85.52% 16.234% 11 16.549 1149 1154 1159 rW2 16362 30979 0.21% 0.041% 12 18.341 1305 1311 1315 rBV 6833629“ 13563239 93.60% 17.768% 13 19.985 1445 1455 1459 rVB2 7400 31235 0.22% 0.041% 14 22.280 1651 1656 1661 rVB 54823 101559 0.70% 0.133% 15 22.645 1681 1688 1693 rBV2 6485545 14490042 100.00% 18.982% 16 22.771 1697 1699 1719 rVB 83268 234038 1.62% 0.307% 17 27.726 2129 2133 2139 rW 835729 1491988 10.30% 1.954% 18 30.500 2369 2376 2381 rBV 5117968 12714680 87.75% 16.656% 19 31.105 2423 2429 2437 rBV4 9075 28980 0.20% 0.038% 20 34.416 2713 2719 2753 rBV 3964662 10822820 74.69% 14.178%

Sum of corrected areas: 76336254

10168.D SCAN508.M Fri Jan 25 10:25:52 2002 Page 1

NYC-WTC_000050504

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NYC-WTC_000050504Source: NYC Law Department, mirrored locally

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