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GCMS analysis results for sample AD31676, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31676 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050317–000050333

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN23\31676.D Vial: 1 Acq On : 23 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rVB 27595 46464 0.09% 0.041% 2 4.241 71 76 83 rBV2 21958 52492 0.10% 0.046% 3 4.355 83 86 93 rVB2 16634 35102 0.07% 0.031% 4 9.710 551 555 561 rBV 3335528 6499486 12.96% 5.733% 5 13.192 855 860 865 rBV 5083718 9284727 18.51% 8.189% 6 18.341 1305 1311 1315 rBV 5190169 10223558 20.39% 9.018% 7 18.741 1339 1346 1359 rBV2 80095 784065 1.56% 0.692% 8 20.876 1519 1533 1535 rBV3 5134 33547 0.07% 0.030% 9 20.933 1535 1538 1547 rW4 19459 59019 0.12% 0.052% 10 22.280 1651 1656 1661 rBV2 45446 84060 0.17% 0.074% 11 22.645 1681 1688 1693 rBV 5074161 11262647 22.46% 9.934% 12 22.851 1695 1706 1731 rVB2 243657 2444024 4.87% 2.156% 13 23.456 1745 1759 1763 rBV5 27851 167872 0.33% 0.148% 14 23.719 1775 1782 1787 rVB4 14440 67028 0.13% 0.059% 15 23.856 1787 1794 1799 rBV6 8514 41686 0.08% 0.037% 16 24.860 1877 1882 1887 rBV 163088 346528 0.69% 0.306% 17 26.150 1977 1995 1999 rVB2 6849919 50149481 100.00% 44.234% 18 27.726 2129 2133 2139 rBV 938932 1685195 3.36% 1.486% 19 30.500 2369 2376 2381 rBV 4286067 10817845 21.57% 9.542% 20 34.416 2713 2719 2755 rBV 3409452 9289600 18.52% 8.194%

Sum of corrected areas: 113374426

31676.D SCAN508.M Thu Jan 24 09:57:32 2002 Page 1

NYC-WTC_000050321

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NYC-WTC_000050321Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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