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GCMS analysis results for sample AD31674, Jan 25 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31674 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050276–000050293

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02JAN22\31674.D Vial: 2 Acq On : 22 Jan 2002 3:30 pm Operator: 'Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rVB2 42537 66504 0.10% 0.046% 2 4.378 83 88 91 rW2 22056 45230 0.07% 0.031% 3 5.006 141 143 147 rBV 33049 55083 0.08% 0.038% 4 9.710 551 555 561 rW 4450423 8393416 12.23% 5.766% 5 9.847 561 567 573 rW2 15905 51273 0.07% 0.035% 6 12.541 799 803 807 rVB 159367 254541 0.37% 0.175% 7 13.192 855 860 865 rBV 6277454 11979845 17.45% 8.230% 8 18.341 1305 1311 1315 rBV 6302433 12898128 18.79% 8.861% 9 18.752 1339 1347 1349 rBV3 112345 447645 0.65% 0.308% 10 22.280 1651 1656 1661 rBV2 61608 112180 0.16% 0.077% 11 22.645 1681 1688 1693 rBV2 6057007 13635283 19.86% 9.367% 12 22.851 1695 1706 1739 rVB2 321376 3352480 4.88% 2.303% 13 23.490 1747 1762 1769 rBV4 40431 326519 0.48% 0.224% 14 23.753 1775 1785 1791 rBV4 27808 145405 0.21% 0.100% 15 24.860 1877 1882 1885 rBV 188119 405149 0.59% 0.278% 16 26.185 1977 1998 2003 rVB 7753725 68651782 100.00% 47.164% 17 27.726 2129 2133 2139 rBV 1115451 2022123 2.95% 1.389% 18 29.667 2299 2303 2325 rVB4 10950 64358 0.09% 0.044% 19 30.500 2369 2376 2381 rBV 4914048 12479145 18.18% 8.573% 20 34.416 2713 2719 2751 rBV 3692007 10174385 14.82% 6.990%

Sum of corrected areas: 145560474

31674.D SCAN508.M Thu Jan 24 14:00:11 2002 Page 1

NYC-WTC_000050280

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NYC-WTC_000050280Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000003981

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.997

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