GCMS analysis results for sample AE00167, Jan 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN24\00167.D Vial: 4 • Acq On : 24 Jan 2002 2:09 pm Operator: •Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.49 0.28 ug/L 136162 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW Mol Form . CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 64 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 59 Abundance Scan 10 (3.488 min): 00167.D (-) m/z 74.00 100.00% 74

82 5000

38 47 ...A...... 3.50 3.60 3.70 3.80 3.90 1 i i 1 > > > । * । ■ ■ i • i rl ■ । ,II > ■ ■ ■ m/z 81.90 49.79% i ■ dit I 1 । । • * 1 l > 1 > ■ r» i miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 82 • • ।1 ■ ■ ■ । ■ • ■ • । ' i ■1' • । ■ 3.50 3.60 3.70 3.80 3.90 47 m/z 83.90 36.92% 35

miz-> ,ri1 * * ■ i • •••i' * * ’ i • • •1।* *• ■ i ' • ■ ■ i ■ 10 20 30 40 50 60 70 80 i TII ।..... 90 1111991 100 110 Abundance #11644: Acetonitrile, dichloro-

35 74 ............ J 3.60 3.70 3.80 3.90 3.50 5000 82 m/z 76.00 33.03% 47

■ ' i ‘ ‘ ■ i ■ ‘ ■ i ■ ■ 1 1 1 • 11 ■ ■ ■ ■ । ■ ■ ■ ■ । ■ "T-1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ iz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... ■b i1 ■ ■ ■ i ■ ■ ■ • i1 ■1 ■ i • • ■ ■ i ■ ■ 74 82 3.50 3.60 3.70 3.80 3.90 m/ Z 47.00 22.58%

5000 47 35

m/z-> 12 *WTIUITI - 10 20 30 40 ■ lr 50 ....60. ...... 70 ' "IiB 80 T-j-T-r-r-r-p-r-r-r-j-TT 90 100 108 110 N \ ' * I • ‘ ' • ! • ‘1 ’ I ‘ 3.50 3.60 370 3.80 3.90 A ‘ ‘ r1 —A

)0167.D SCAN508.M Fri Jan 25 10:25:46 2002 Page 3

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