Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
NYC-WTC_000050444–000050480Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\l\5973N\02JAN25\0104B2.D vial: 4 * Acq On : 25 Jan 2002 12:39 pm Operator: Sample : lab blank 1/4; 2nd inj. Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Cyclopentasiloxane, decamet... Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
12.54 0.05 ug/L 22119 Naphthalene-d8 13.19
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Amodiaquine $$ Phenol, 4-[(7-chl... 355 C20H22C1N30 000086-42-0 9 3 IIH-Dibenzo[b,E][1,4]diazepin-11... 267 C16H17N3O 013450-73-2 5 4 1,3-Benzodioxole-5-ethanamine, 6... 355 C21H25NO4 050657-26-6 4 Abundance Scan 803 (12.541 min): 0104B2.D (-) m/z 73.10 100.00% 73
5000 267 355 • ■ i ■ ■ ■ ■ i 1 ■ i ■ 1 ‘ ■ i ■ ■ ■ ■ i ■ 12.20 12.40 12.60 12.80 — miz—> I“••l 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 —T m/z 267.00 36.70% Abundance #313065: Cyclopentasiloxane, decamethyl- 73
5000 267 ■ ■ i ■ ■ ■ • i • ■ । • • •1 । ■ • • ■ ।1 12.20 12.40 12.60 12.80 355 m/z 355.10 29.36% 45 193 223 251 , i' ■ ■ ■ i ■ ■ “ i ■'1 ■ i ■ ■" i “ ■ ■ i “ । ■ i ■ ■ “ । n li (i^up 11 Ai । iTu 11 ■ miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #302438: Amodiaquine $$ Phenol, 4-[(7-chloro-4-quinoliny!)... 58 - 282 ■ ■ i ■ ■ 1 ■ i ' 1 12.20 12.40 12.60 12.80 5000 m/z 267.90 14.81% 73 355 218 253 170 191 1 I' ‘‘ I /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #209481:11 H-Dibenzo[b,E][1,4]diazepin-11-one, 5-(3-aminop... 30 118 12.20 12.40 12.60 12.80 77 267 m/z 357.10 9.54% 181 223 238 5000 52 । • i * •1 • । • i1 ■111'1' ■ ' “ i ■ ■ ■11 ■" ■ THT—gT] " ■ ‘ i • " ■ i " " r ‘ “ i' ■ ■ ‘ i ■ miz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.20 12.40 12.60 12.80
104B2.D SCAN508.M Fri Jan 25 13:22:50 2002 Page 10
NYC-WTC_000050474
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050627
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on February 4-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052233
Laboratory report showing GCMS blank analysis of sample AE00842 with compounds below detection limits.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051531
Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051674
Laboratory report showing GCMS blank analysis results for sample AE00365 conducted between January 15 and 16, 2002.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003425
Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.
2 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006026
Laboratory report documenting a GCMS blank test for sample AE03184 conducted on March 6, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006065
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000003503
Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
Filed in the same folder