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GCMS analysis results for sample AD31675, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AD31675 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050294–000050316

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data.File : C:\MSDCHEM\l\5973N\02JAN24\31675A.D Vial: 2 Acq On : 24 Jan 2002 12:31 pm Operator: Sample : 508scan; re-inj Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.613 17 21 25 rBV 37530 67677 0.12% 0.051% 2 4.253 71 77 83 rW3 21800 59657 0.11% 0.045% 3 9.413 525 529 535 rW 61370 124919 0.23% 0.094% 4 9.710 551 555 561 rW 4078393 8362916 15.30% 6.270% 5 12.541 799 803 807 rBV 77173 134458 0.25% 0.101% 6 13.192 855 860 865 rBV 6064602 11972886 21.90% 8.977% 7 18.341 1305 1311 1315 rBV 6551871 12997127 23.77% 9.744% 8 18.855 1339 1356 1363 rBV5 89505 1121229 2.05% 0.841% 9 20.933 1523 1538 1547 rVB4 14505 84607 0.15% 0.063% 10 21.618 1589 1598 1607 rVB5 8980 68310 0.12% 0.051% 11 22.280 1651 1656 1661 rBV 60694 117825 0.22% 0.088% 12 22.645 1681 1688 1693 rW 6313371 13917013 25.46% 10.434% 13 22.851 1695 1706 1733 rVB2 257561 2594033 4.74% 1.945% 14 23.433 1745 1757 1765 rBV2 32960 176620 0.32% 0.132% 15 23.696 1769 1780 1785 rBV6 26510 149615 0.27% 0.112% 16 24.860 1877 1882 1887 rBV 186692 405828 0.74% 0.304% 17 26.139 1977 1994 1999 rVB 7869866 54671113 100.00% 40.989% 18 27.726 2127 2133 2139 rBV 1166327 2116185 3.87% 1.587% 19 30.500 2369 2376 2381 rBV 5267673 12990976 23.76% 9.740% 20 34.416 2713 2719 2749 rBV 4148573 11246204 20.57% 8.432%

Sum of corrected areas: 133379198

31675A.D SCAN508.M Thu Jan 24 15:25:29 2002 Page 1

NYC-WTC_000050302

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NYC-WTC_000050302Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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