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GCMS analysis results for sample AE00107, Feb 13 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00107 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050145–000050154

Folder label: “GCMS X 1/3/02 A 1/24/02

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Scanned page image, NYC-WTC_000050150
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN2402\107.D Vial 14 Acq On : 25 Jan 2002 1:49 am Operator 209 GALOS Sample : GC/MS SCAN 1/3 Inst GC/MS 209 Mise : Multiplr 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks’: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.434 256 260 295 rVB 292544 913026 13.20% 2.571% 2 11.483 696 701 721 rBV 2048461 5334811 77.11% 15.022% 3 14.127 984 989 996 rBV 154914 308895 4.46% 0.870% 4 15.081 1087 1093 1111 rBV 3271855 6766534 97.80% 19.054% 5 20.342 1660 1666 1690 rBV 3331569 6918586 100.00% 19.482%

6 24.757 2141 2147 2159 rBV2 3009882 6450319 93.23% 18.163% 7 29.834 2695 2700 2708 rBV 382788 725050 10.48% 2.042% 8 32.781 3015 3021 3037 rBV2 1913624 4578827 66.18% 12.893% 9 36.848 3456 3464 3486 rBV 1287402 3516902 50.83% 9.903%

Sum of corrected areas: 35512950

107.D GCMS0208.M Fri Feb 08 13:38:41 2002

NYC-WTC_000050150

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NYC-WTC_000050150Source: NYC Law Department, mirrored locally

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