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GCMS analysis results for sample AD31673, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31673 including unknown compounds and surrogate recovery data.

NYC-WTC_000050053–000050065

Folder label: “GCMS X 1/3/02 A 1/17/02

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NYC 9/11 Public Portal Document LC Area PerceIC Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31673 .D Vial: 8 • Acq On : 17 Jan 2002 8:39 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rBV 39329 56405 0.49% 0.091% 2 4.367 85 87 95 rVB 13895 25133 0.22% 0.040% 3 4.618 107 109 117 rVB2 21116 36545 0.32% 0.059% . 4 4.835 125 128 137 rBV2 26522 68683 0.60% 0.110% 5 5.006 139 143 149 rVB2 13855 26055 0.23% 0.042%

6 5.885 217 220 245 rBV 772347 1627691 14.28% 2.615% 7 9.710 551 555 561 rW 3560069 6594197 57.83% 10.595% 8 9.858 561 568 577 rW2 7951 30131 0.26% 0.048% 9 10.110 585 590 595 rVB3 7690 20146 0.18% 0.032% 10 12.541 799 803 807 rVB 19615 35913 0.31% 0.058% 11 13.192 855 860 865 rBV 5101035 9523863 83.53% 15.302% 12 18.341 1305 1311 1315 rBV 5335576 10589412 92.87% 17.014% 13 22.280 1653 1656 1661 rBV2 39828 73843 0.65% 0.119% 14 22.645 1681 1688 1693 rBV2 5007657 11401817 100.00% 18.320% 15 22.771 1695 1699 1713 rVB 62183 181159 1.59% 0.291% 16 24.849 1877 1881 1891 rBV 85436 157025 1.38% 0.252% 17 27.726 2127 2133 2139 rBV 835458 1475559 12.94% 2.371% 18 30.500 2369 2376 2381 rBV 4433448 10827209 94.96% 17.396% 19 31.105 2419 2429 2437 rBV4 16484 62488 0.55% 0.100% 20 34.416 2713 2719 2765 rBV 3662055 9424706 82.66% 15.143%

Sum of corrected areas: 62237980

31673.D SCAN508.M Tue Jan 22 08:37:33 2002 Page 1

NYC-WTC_000050057

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NYC-WTC_000050057Source: NYC Law Department, mirrored locally

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