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GCMS analysis results for sample AD31638, Jan 28 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AD31638 including unknown compounds and surrogate recovery data.

NYC-WTC_000049944–000049956

Folder label: “GCMS X 1/3/02 A 1/17/02

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Scanned page image, NYC-WTC_000049948
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NYC 9/11 Public Portal Document LbU area Percent Report

Data File : C:\MSDCHEM\1\5973N\02JAN17\31638.D Vial: 5 ' Acq On : 17 Jan 2002 1:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.602 17 20 25 rW 22912 32295 0.30% 0.056% 2 3.750 31 33 45 rW4 4287 17603 0.16% 0.031% 3 3.990 49 54 59 rW4 8284 18289 0.17% 0.032% 4 4.241 73 76 79 rBV2 9987 18683 0.17% 0.032% 5 4.367 83 87 91 rVB 17464 30022 0.28% 0.052% 6 4.630 107 110 117 rVB3 10393 24043 0.22% 0.042% 7 4.835 123 128 139 rBV5 19794 56273 0.52% 0.098% 8 5.509 183 187 203 rVB6 7255 35093 0.33% 0.061% 9 5.885 217 220 247 rVB 537856 1167899 10.86% 2.031% 10 9.425 527 530 537 rBV2 6155 16929 0.16% 0.029% 11 9.710 551 555 561 rBV 3147755 6319513 58.76% 10.988% 12 13.192 855 860 865 rBV 4768928 9040847 84.06% 15.720% 13 18.341 1305 1311 1315 rBV 5121843 9965298 92.65% 17.327% 14 22.280 1653 1656 1661 rW2 40641 76442 0.71% 0.133% 15 22.645 1681 1688 1693 rW2 4688645 10755702 100.00% 18.701%

16 22.771 1695 1699 1721 rW 63141 210091 1.95% 0.365% 17 24.849 1877 1881 1887 rBV 71528 127765 1.19% 0.222% 18 27.726 2127 2133 2139 rBV 730357 1257471 11.69% 2.186% 19 30.489 2369 2375 2381 rBV2 4194047 10059035 93.52% 17.490% 20 34.416 2713 2719 2747 rBV 3262216 8284203 77.02% 14.404%

Sum of corrected areas: 57513496

31638.D SCAN508.M Tue Jan 22 08:37:01 2002 Page 1

NYC-WTC_000049948

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NYC-WTC_000049948Source: NYC Law Department, mirrored locally

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