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GCMS analysis results for sample AE00110, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00110 analyzed on February 13, 2002.

NYC-WTC_000050645–000050663

Folder label: “GCMS X 1/4/02 A 2/4/02

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NYC 9/11 Public Portal Document LbC area Percent Report Data File : C:\MSDCHEM\1\5973N\02FEB04\00110.D Vial: 4 • Acq On : 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\SCAN508.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total

1 3.602 17 20 25 rBV 29995 45842 0.26% 0.048% 2 4.241 73 76 83 rBV4 25928 61987 0.35% 0.065% 3 4.618 107 109 121 rW3 22220 58156 0.33% 0.061% 4 4.835 125 128 141 rW2 41049 125028 0.71% 0.130% 5 5.006 141 143 147 rVB 26720 47945 0.27% 0.050%

6 5.885 217 220 243 rW 661227 1479341 8.40% 1.544% 7 9.538 535 540 545 rW 44589 99246 0.56% 0.104% 8 9.630 545 548 551 rW 51909 110782 0.63% 0.116% 9 9.710 551 555 561 rW 5096440 10593339 60.17% 11.056% 10 9.835 561 566 587 rVB 58063 203371 1.16% 0.212%

11 13.203 855 861 865 rBV 7210448 15021696 85.32% 15.677% 12 16.548 1149 1154 1159 rVB 26538- 48732 0.28% 0.051% 13 18.341 1305 1311 1317 rBV 7771849 16377088 93.02% 17.092% 14 22.280 1653 1656 1661 rBV 78533 145678 0.83% 0.152% 15 22.645 1681 1688 1693 rBV2 7598406 17605750 100.00% 18.374%

16 22.771 1697 1699 1713 rVB 109433 299651 1.70% 0.313% 17 27.726 2129 2133 2139 rBV 1050880 1895967 10.77% 1.979% 18 30.500 2369 2376 2381 rBV2 6386654 16836066 95.63% 17.571% 19 31.105 2423 2429 2447 rVB 56075 230676 1.31% 0.241% 20 34.427 2713 2720 2749 rBV 5029558 14533060 82.55% 15.167%

Sum of corrected areas: 95819401

>0110.D SCAN508.M Tue Feb 05 09:47:00 2002 Page 1

NYC-WTC_000050649

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