GCMS analysis results for sample AD31637, Jan 28 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN17\31637.D Vial: 4 Acq On : 17 Jan 2002 12:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 1,3,5-Cycloheptatriene (CAS... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.37 0.10 ug/L 32854 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3,5-Cycloheptatriene (CAS) $$ ... 92 C7H8 000544-25-2 80 2 Benzene, methyl- (CAS) $$ Toluen... 92 C7H8 000108-88-3 72 3 Benzene, methyl- (CAS) $$ Toluen... 92 C7H8 000108-88-3 72 4 Toluene 92 C7H8 000108-88-3 72 Abundance Scan 87 (4.367 min): 31637. D (-) m/z 91.10 100.00% 91

5000

■ ' i ■ ■ ' ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ ■ • ■ i 1 39 43 47 51 65 85 4.00 4.20 4.40 4.60 4.80 0h --- - Hpopper m/z 92.00 67.95% nz-> 25 3035404550556065 70 75 80 85 90 95 100 Abundance #5573:1,3,5-Cycloheptatriene (CAS) $$ Cycloheptatriene 9h % 5000 ■ ■ i ■ ■ ' ‘ i ■ ■ • • i • ■ • ■ i • ■ ■ ■ i ■ 4.00 4.20 4.40 4.60 4.80 65 m/z 65.00 12.71% 46 51 78 Oh —mmmmmmn—r mmmTH i • । •»• • । • niz-> 25 3035404550556065 70 75 80 85 90 95 100 Abundance #5544: Benzene, methyl- (CAS) $$ Toluene $$ CP 25 $$ Methy... 91 ■ ■ । ■1 ■ ।' ■ ■ ■ । • ■ ■ • । ■ • ■ ■ ।1 4.00 4.20 4.40 4.60 4.80 5000 m/z 39.10 8.38% 65 . 51। 85 35 46 Oh -IPmmmHtmm] 1 ■ ■ ■ i ■ ■ ■ ■ i1 ■ ■ ■ i ■ —H+ I > 111»• 1«• miz-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5539: Benzene, methyl- (CAS) $$ Toluene $$ CP 25 $$ Methy... 91 .00. 4.00 4.20 4.40 4.60 4.80 m/z 51.00 7.59% 5000 wWWWw/ 45 51 6165 Oh ■■i “ ■•i'1111■"'11"11'11■i■■■■i11'1111111 ■■ “ i'' ■1 i1 ■ ■ ■ i ■ ■ ■ H 4-r-j-rrrrp-r ■ ■ i 1 ■ ' ' i ■ ■ 1 ' i 1 ■ ■ • i ■ ■ ■ ■ i 1 n/z—> 25 30 35 40 4550556065 70 75 808590 95 100 4.00 4.20 4.40 4.60 4.80

31637.D SCAN508.M Tue Jan 22 08:36:58 2002 Page 5

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