GCMS analysis results for sample AD31585, Jan 17-22 2002

NYC 9/11 Public Portal Document yuaxicxc.au ion keport (NOC Kevlewed)

Data File : C:\MSDCHEM\1\5973N\02JAN17\0103R.D Vial: 2 • Acq On : 17 Jan 2002 11:01 am Operator: Sample : ref 1/3 Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: SPLIT.P Quant Time: Jan 22 08:29:59 2002 Quant Results File: SCAN508.RES Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Last Update : Fri Jan 11 13:20:07 2002 Response via : Initial Calibration DataAcq Meth : SCAN508 Internal Standards R.T. Qlon Response Cone Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 9.72 152 1022413 20.00 ug/L 0.00 10) Naphthalene-d8 13.19 136 4361982 20.00 ug/L -0.02 17) Acenaphthene-diO 18.34 164 2356670 20.00 ug/L -0.01 29) Phenanthrene-diO 22.63 188 4050793 20.00 ug/L -0.03 38) Chrysene-dl2 30.50 240 3586919 20.00 ug/L -0.01 44) Perylene-dl2 34.42 264 2611034 20.00 ug/L 0.00 System Monitoring Compounds 37) 2,4-DDD 27.73 235 310500 4.85 ug/L 0.00 Spiked Amount 5.000 Recovery = 97.00% Target Compounds Qvalue 2) n-Nitrosodimethylamine 3.99 74 128652 2.95 ug/L 49 3) bis(2-Chloroethyl)ether 9.24 93 277843 3.91 ug/L 70 4) 1,3-Dichiorobenzene 9.61 146 204242 2.66 ug/L 96 5) 1,4-Dichlorobenzene 9.76 146 208952 2.71 ug/L 97 6) 1,2-Dichlorobenzene 10.24 146 215698 3.15 ug/L 96 7) 2,2'-oxybis (1-Chloropropa 10.67 45 390214 3.30 ug/L # 73 8) n-Nitroso-di-n-propylamine 11.06 70 190572 3.53 ug/L 75 9) Hexachioroethane 11.03 117 53313 1.93 u§/L 98 11) Nitrobenzene 11.35 77 219738 2.70 ug/L 86 12) 1sophorone 12.03 82 542814 3.69 ug/L 91 13) bis(2-Chloroethoxy)methane 12.77 93 346800 3.97 ug/L 92 14) 1,2,4-Trichiorobenzene 13.11 180 167776 2.95 ug/L 97 15) Naphthalene 13.25 128 776534 3.72 ug/L 99 16) Hexachlorobutadiene 13.84 225 55563 1.84 ug/L 99 18) Hexachlorocyclopentadiene 15.95 237 8245 0.39 ug/L 98 19) 2-Chloronaphthalene 16.65 162 443432 3.41 ug/L 93 20) Dimethylphthalate 17.88 163 611355 3.93 ug/L 93 21) 2,6-Dinitrotoluene 18.06 165 69140 2.28 ug/L 85 2 2) Acenaphthylene 17.86 152 711004 3.75 ug/L 97 2 3) Acenaphthene 18.42 153 518864 3.84 ug/L 96 24) 2,4-Dinitrotoluene 19.17 165 80873 2.03 ug/L 95 25) Diethylphthalate 20.00 149 642580 4.31 ug/L 98 26) 4-Chlorophenyl-phenylether 20.02 204 277920 4.43 ug/L 86 27) Fluorene 19.91 166 631669 4.11 ug/L 96 2 8) Azobenzene/1,2-Diphenylhyd 20.46 77 683384 3.68 ug/L 83 30) N-nitrosodiphenylamine 20.43 169 322462 3.14 ug/L 98 31) 4-Bromophenyl-phenylether 21.44 248 166566 3.95 ug/L 90 3 2) Hexachlorobenzene 21.77 284 170646 3.83 ug/L 97 3 3) Phenanthrene 22.70 178 1006670 4.51 ug/L 99 3 4) Anthracene 22.82 178 926199 4.28 ug/L 98

(#) = qualifier out of range (m) = manual integration 0103R.D SCAN508.M Tue Jan 22 08:30:00 2002 Page 1

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