GCMS reference results for sample AD29228, January 2002

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Quantitation Report Reviewed)

Data File C:\HPCHEM\1\DATA\JANO3O2\LB .D 0 Vial: 18 Acq On 4 Jan 2002 3:08 am Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 3:56 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.52 152 743282 20.00 ug/1 -0.18 10) Naphthalene-d8 15.12 136 2892354 20.00 ug/1 -0.18 17) Acenaphthene-diO 20.39 164 1443340 20.00 ug/1 -0.18 29) Phenanthrene-diO 24.81 188 1951754 20.00 ug/1 -0.18 38) Chrysene-dl2 32.83 240 1064209 20.00 ug/1 -0.20 44) Perylene-dl2 36.90 264 609438 20.00 ug/1 -0.22

System Monitoring Compounds 37) 2,4-DDD 29.88 235 108107 5.04 ug/mL -0.19 Spiked Amount 5.000 Recovery = 100.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 187 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachioroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.84 77 181 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 2813 N.D. 16) Hexachiorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 21.91 149 7067 N.D. 26) 4-Chlorophenyl-phenylether • 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0103.M Thu Jan 10 12:10:44 2002 Page 1

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