GCMS calibration results for sample AD29228, January 2002

NYC 9/11 Public Portal Document Quantitation Report

Data File : C:\HPCHEM\1\DATA\JAN0302\REF.D Acq On . Sample Mise : 4 Jan 2002 : gems scan 1/2 4:06 am w (Net /Reviewed)

Vial: Operator: Inst Multiplr: : 19 209 GALOS GC/MS 209 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 4:55 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.53 152 684216 20.00 ug/1 -0.17 10) Naphthalene-d8 15.12 136 2708192 20.00 ug/1 -0.19 17) Acenaphthene-diO 20.39 164 1340401 20.00 ug/1 -0.19 29) Phenanthrene-diO 24.80 188 1872732 20.00 ug/1 -0.19 38) Chrysene-dl2 32.84 240 1095991 20.00 ug/1 -0.20 44) Perylene-dl2 36.90 264 639378 20.00 ug/1 -0.22

System Monitoring Compounds 37) 2,4-DDD 29.88 235 102967 5.00 ug/mL -0.19 Spiked Amount 5.000 Recovery = 100.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.30 74 75783 2.52 ug/1 # 68 3) bis(2-Chloroethyl)ether 10.96 93 182502 3.86 ug/1 # 88 4) 1,3-Dichlorobenzene 11.43 146 82481 1.66 ug/1 99 5) 1,4-Dichlorobenzene 11.57 146 93299 1.85 ug/1 # 97 6) 1,2-Dichlorobenzene 12.08 146 98558 2.12 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 12.43 45 303945 5.05 ug/1 # 91 8) N-Nitroso-di-n-propylamine 12.80 70 123913 4.61 ug/1 # 88 9) Hexachloroethane 12.91 117 18245 1.00 ug/1 93 11) Nitrobenzene 13.20 77 169442 4.01 ug/1 # 83 12) Isophorone 13.84 82 351168 4.32 ug/1 # 91 13) bis(2-Chloroethoxy)methane 14.54 93 224196 4.10 ug/1 99 14) 1,2,4-Trichlorobenzene 15.02 180 81421 2.07 ug/1 94 15) Naphthalene 15.17 128 415784 3.21 ug/1 99 16) Hexachlorobutadiene 15.73 225 11239 0.59 ug/1 96 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.66 162 221313 2.89 ug/1 95 20) Dimethylphthalate 19.78 163 334279 3.75 ug/1 99 21) 2,6-Dinitrotoluene 19.98 165 53616 2.55 ug/1 # 57 2 2) Acenaphthylene 19.92 152 348518 3.24 ug/1 100 23) Acenaphthene 20.48 153 267032 3.48 ug/1 99 24) 2,4-Dinitrotoluene 21.15 165 62221 2.33 ug/1 # 59 25) Diethylphthalate 21.90 149 344018 4.17 ug/1 97 26) 4-Chlorophenyl-phenylether 22.03 204 123248 3.42 ug/1 # 89 27) Fluorene 21.99 166 282724 3.59 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.50 77 330155 3.88 ug/L # 89

(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Thu Jan 10 12:12:01 2002 Page 1

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