Calibration data report for GCMS analysis of sample AD29228 generated on January 3, 2002.
NYC-WTC_000049782–000049786Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN0302\REF.D Vial: 19 Acq On : 4 Jan 2002 4:06 am Operator: 209 GALOS Sample : gems scan 1/2 Inst : GC/MS 209 Mise ■ Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 4:55 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Compound R.T. Qlon Response Cone Unit Qvalue
30) N-Nitrosodiphenylamine 22.43 168 94880 2.85 ug/1 # 74 31) 4-Bromophenyl-phenylether 23.49 248 65314 3.55 ug/1 93 32) Hexachlorobenzene 23.90 284 66882 3.30 ug/1 94 3 3) Phenanthrene 24.87 178 393022 3.96 ug/1 98 3 4) Anthracene 25.01 178 330670 3.34 ug/1 100 35) Di-n-butylphthalate 26.82 149 515406 3.91 ug/1 # 99 36) Fluoranthene 28.48 202 348749 3.64 ug/1 99 3 9) Pyrene 29.15 202 361618 3.82 ug/1 97 40) Butylbenzylphthalate 31.33 149 161033 3.26 ug/1 # 85 41) Benzo(a)anthracene 32.78 228 232305 3.56 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.13 149 200810 3.01 ug/1 97 43) Chrysene 32.91 228 260238 4.06 ug/1 99 45) Di-n-Octylphthalate 34.87 149 204232 2.40 ug/1 # 87 46) Benzo(b)fluoranthene 35.86 252 176151 3.66 ug/1 99 47) Benzo(k)fluoranthene 35.92 252 212870 4.31 ug/1 98 4 8) Benzo(a)pyrene 36.73 252 125231 2.99 ug/1 96 4 9) Indeno(1,2,3-cd)pyrene 40.47 276 127665 3.05 ug/1 96 50) Dibenz(a,h)anthracene 40.54 278 111791 3.41 ug/1 95 51) Benzo(g,h,i)perylene 41.53 276 120726 3.38 ug/1 # 90
(#) = qualifier out of range (m) = manual integration REF.D GCMS0103.M Thu Jan 10 12:12:05 2002 Page 2
NYC-WTC_000049785
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NYC-WTC_000049679
Laboratory report of GCMS reference analysis for sample AD31586 listing chemical standards and response values.
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Calibration report for GCMS analysis of sample AE00005 listing target compounds and response factors.
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Reference standard analysis data verifying instrument performance for detecting volatile organic compounds in water samples.
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Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.
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Reference analysis report for DEP sample AD31432 listing results for volatile organic compounds from January 18, 2002.
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Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
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GCMS reference analysis report for sample AD31129 listing component names and values from January 10, 2002.
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Laboratory report of gas chromatography-mass spectrometry reference analysis performed on January 16, 2002.
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Reference standard analysis report for GCMS testing verifying instrument performance with specific compound concentrations on February 21, 2002.
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Reference standard analysis showing response factors for organic compounds from February 2002.
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Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
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