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GCMS analysis results for sample AD31633, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31633 conducted on February 11, 2002.

NYC-WTC_000049713–000049722

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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Scanned page image, NYC-WTC_000049718
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C: \HPCHEM\ 1 \DATA\JANO 302\31633.D Vial: 40 Acq On 5 Jan 2002 12:31 am Operator: 209 GALOS Sample gems scan 1/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.464 260 264 298 rVB 360563 1063070 18.66% 3.717% 2 11.522 701 706 724 rBV 1688865 4347925 76.32% 15.202% 3 14.166 989 994 999 rBV2 62563 117190 2.06% 0.410% 4 15.120 1093 1098 1117 rBV 2713834 5560957 97.62% 19.444% 5 20.390 1666 1672 1687 rBV 2750534 5696784 100.00% 19.919%

6 24.806 2147 2153 2164 rBV2 2481929 5305864 93.14% 18.552% 7 29.882 2701 2706 2712 rBV 357379 678992 11.92% 2.374% 8 32.829 3021 3027 3049 rBV2 1494113 3468527 60.89% 12.128% 9 36.896 3463 3470 3487 rBV2 834621 2361140 41.45% 8.256%

Sum of corrected areas: 28600449

31633.D GCMS1126.M Fri Feb 01 11:12:55 2002

NYC-WTC_000049718

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NYC-WTC_000049718Source: NYC Law Department, mirrored locally

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