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GCMS analysis results for sample AD30983, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AD30983 performed on 1/25/02, detecting 2,4-DDD compound at 101 micrograms with 5.0 MDL.

NYC-WTC_000018238–000018247

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018243
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\1\DATA\DEC3101\30983.D Vial: 37 Acq On 1 Jan 2002 11:49 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF• Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.617 276 280 297 rBV 236215 779607 13.74% 2.866% 2 11.675 717 722 740 rBV 1485272 4083919 71.98% 15.011% 3 15.283 1109 1115 1139 rBV 1695632 5145275 90.68% 18.913% 4 20.561 1684 1690 1705 rBV 1982961 5674003 100.00% 20.856% 5 24.986 2166 2172 2218 rBV2 1317052 5273029 92.93% 19.382%

6 30.072 2720 2726 2738 rBV 259805 643710 11.34% 2.366% 7 33.028 3041 3048 3063 rBV2 1037339 3405383 60.02% 12.517% 8 33.175 3063 3064 3066 rVB 100539 58134 1.02% 0.214% 9 37.123 3487 3494 3524 rBV2 486493 2142371 37.76% 7.875% v

Sum of corrected areas: 27205431

30983.D GCMS1126.M Wed Jan 23 08:51:32 2002

NYC-WTC_000018243

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NYC-WTC_000018243Source: NYC Law Department, mirrored locally

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