GCMS analysis results for sample AE08962, May 7, 2002

NYC 9/11 Public Portal Document JJL{*y DCCLit UILpUulic A\SD —

Data File : C:\MSDCHEM\1\DATA\020424\08962.D Vial: 13 Acq On : 24 Apr 2002 9:39 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ******************** ************************************************* Peak Number 1 Methane, bromodichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.35 0.34 ug/1 384849 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Methane, bromodichloro- 162 CHBrC12 000075-27-4 86 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 80 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 4 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 72 Abundance Scan 46 (3.349 min): 08962.D (-42) (-) m/z 83.00 100.00% 83

5000

47 35 TfWprepur D 158.. . 191..................... . 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 85.00 68.52% niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

5000 w meym > hmmpmmm Amm 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/z47.10 13 27 35 |||, 116 ||. 63 72 1. | _ 164 93 129 If I fl I J | II l ! | J I J*l | ) I II I I I I I' l ! ! "p | l I ri’f'ri ftM u । rm । rm p j ihyi 11 q n 111 > । > 11’1 iipn niz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116497: Methane, bromodichloro- 83 Wwv 11—8811100—*" 3.20 3.30 3.40 3.50 3.60 3.70 3.80 5000 m/z 84.00 17.13%

miz-> 28 , 47— ............. Ill 191. ........ 129 -47 ||. • i • ■ •11 • • *11 *1 1‘1‘—09201111-0119B930101m ——u33T 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 ■ woow Abundance #116506: Methane, bromodichloro- । । <1111111 ■ > i j 1111111 83 3.20 3.30 3.40 3.50 3.60 370 3.80 m/z 87.00 14.40% 5000-

47 129

/z—> ।j।। 13 . 35 Ih, 55 64 72 11,191 116 || 144 163 i »j i r 11 । । I’rs । j । ir ji 111 1 j । 11 in 11 i l 11 Itli > 11 i j j H it rsgrtt 11 j 11 i 1 j 111 ri 1 1*tT v । t i r 10 20 30 40 50 K) 70 80 90 100 110 120 130 140 150 160 170 MAAAMAA-mpApoaA, 3.20 3.30 3.40 3.50 3.60 3.70 3.80

08962.D SCAN020424.M Thu May 02 14:47:49 2002 Page 3

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