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GCMS results for sample AE09092, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09092 conducted on April 30, 2002.

NYC-WTC_000049493–000049507

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049501
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9092.D Vial: 23 . Acq On : 26 Apr 2002 1:42 pm Operator: Sample : re-inject Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.365 140 144 150 rBV 28721 56260 1.86% 0.359% 2 8.183 339 342 369 rVB 296309 702917 23.25% 4.480% 3 12.213 775 781 797 rVB 883776 2139945 70.77% 13.640% 4 14.811 1055 1064 1070 rBV 63367 120424 3.98% 0.768% 5 15.839 1171 1176 1190 rBV 1268502 2692939 89.06% 17.165% 6 21.145 1748 1754 1769 rBV 1475333 3023850 100.00% 19.274% 7 23.284 1980 1987 1993 rBV 149621 282340 9.34% 1.800% 8 25.588 2231 2238 2249 rBV 1420038 2893988 95.71% 18.447% 9 32.226 2956 2961 2969 rBV 49865 118484 3.92% 0.755% 10 33.640 3109 3115 3129 rBV2 958341 2148915 71.07% 13.697% 11 37.872 3568 3576 3597 rBV2 507241 1508390 49.88% 9.615%

Sum of corrected areas: 15688452 9092.D GCMS0412.M Fri Apr 26 14:50:20 2002

NYC-WTC_000049501

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NYC-WTC_000049501Source: NYC Law Department, mirrored locally

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