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GCMS results for sample AE09021, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09021 conducted on April 30, 2002.

NYC-WTC_000049452–000049462

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049457
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9021.D Vial: 19 • Acq On : 26 Apr 2002 6:04 am Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.364 139 144 150 rBV 27767 54114 1.68% 0.321% 2 8.181 339 342 368 rBV 266383 672822 20.83% 3.987% 3 12.212 775 781 794 rBV 911679 2240835 69.37% 13.280% 4 14.810 1059 1064 1069 rVB 45771 81659 2.53% 0.484% 5 15.838 1171 1176 1189 rBV 1355136 2865813 88.72% 16.984% 6 21.144 1748 1754 1773 rBV 1620415 3230173 100.00% 19.143% 7 23.283 1980 1987 1994 rVB 152432 295747 9.16% 1.753% 8 25.587 2231 2238 2249 rBV2 1481861 3176873 98.35% 18.827% 9 33.638 3108 3115 3128 rBV2 1098077 2443767 75.65% 14.482% 10 37.871 3567 3576 3591 rBV2 618039 1812194 56.10% 10.740%

Sum of corrected areas: 16873997 9021.D GCMS0412.M Fri Apr 26 11:08:21 2002

NYC-WTC_000049457

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NYC-WTC_000049457Source: NYC Law Department, mirrored locally

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