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GCMS results for sample AE09090, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09090 conducted on April 30, 2002.

NYC-WTC_000049473–000049482

Folder label: “GCMS X 4/16/02 A 4/26/02

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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\APR2502\9090.D Vial: 21 . Acq On : 26 Apr 2002 7:58 am Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.182 339 342 374 rVB 239218 628314 21.82% 4.267% 2 12.213 775 781 797 rBV 798095 2050205 71.19% 13.924% 3 14.811 1057 1064 1069 rVB 30474 56750 1.97% 0.385% 4 15.839 1170 1176 1190 rBV 1248406 2582782 89.68% 17.541% 5 21.145 1748 1754 1771 rBV 1446031 2880094 100.00% 19.561% 6 23.284 1975 1987 1994 rBV 135937 265414 9.22% 1.803% 7 25.588 2231 2238 2249 rBV 1352242 2802372 97.30% 19.033% 8 33.639 3109 3115 3136 rBV2 904707 2031387 70.53% 13.796% 9 37.871 3568 3576 3591 rBV 480125 1426704 49.54% 9.690%

Sum of corrected areas: 14724022 9090.D GCMS0412.M Fri Apr 26 11:08:47 2002

NYC-WTC_000049478

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NYC-WTC_000049478Source: NYC Law Department, mirrored locally

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