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GCMS results for sample AE09091, April 30, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09091 conducted on April 30, 2002.

NYC-WTC_000049483–000049492

Folder label: “GCMS X 4/16/02 A 4/26/02

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Scanned page image, NYC-WTC_000049488
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NYC 9/11 Public Portal Document L*

Data File : C:\HPCHEM\1\DATA\APR2502\9091.D Vial: 22 • Acq On : 26 Apr 2002 12:48 pm Operator: Sample : re-inject Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.188 338 342 373 rVB 243311 622656 21.31% 4.122% 2 12.209 775 780 797 rVB 816840 2054457 70.32% 13.600% 3 14.816 1057 1064 1068 rBV 36738 71520 2.45% 0.473% 4 15.844 1170 1176 1193 rBV 1282946 2597336 88.90% 17.193% 5 21.141 1747 1753 1767 rBV 1417282 2921725 100.00% 19.340% 6 23.280 1979 1986 1992 rBV 125126 256733 8.79% 1.699% 7 25.585 2231 2237 2245 rBV2 1363240 2829959 96.86% 18.733% 8 33.645 3108 3115 3134 rBV 964592 2166106 74.14% 14.339% 9 37.868 3566 3575 3601 rBV2 517712 1586287 54.29% 10.500%

Sum of corrected areas: 15106779 9091.D GCMS0412.M Fri Apr 26 14:50:03 2002

NYC-WTC_000049488

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NYC-WTC_000049488Source: NYC Law Department, mirrored locally

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