GCMS reference data for sample AE08971, April 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR2502\REFA2.D Vial: 16 Acq On : 26 Apr 2002 3:12 am Operator: Sample : re-inject Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 9:30 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.21 152 497907 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1804463 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1015807 20.00 ug/1 -0.02 3 0) Phenanthrene -dl0 25.58 188 1500491 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 1046569 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 646453 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 23.28 209 45495 8.86 ug/L -0.05 Spiked Amount 10.000 Recovery = 88.60% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 111715 10.31 ug/1 96 3) bis(2-Chloroethyl)ether 11.60 93 270616 16.05 ug/1 98 4) 1,3-Dichlorobenzene 12.11 146 185273 10.65 ug/1 98 5) 1,4-Dichiorobenzene 12.25 146 199475 11.40 ug/1 99 6) 1,2-Dichlorobenzene 12.77 146 206751 12.72 ug/1 99 7) 2,2’-oxybis(1-Chloropropan 13.09 45 373550 16.03 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 176803 15.98 ug/1 98 9) Hexachloroethane 13.62 117 41776 6.51 ug/1 95 11) Nitrobenzene 13.89 77 245961 15.55 ug/1 99 12) 1sophorone 14.. 53 82 400742 13.39 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 326894 16.76 ug/1 100 14) 1,2,4-Trichiorobenzene 15.73 180 184913 13.48 ug/1 99 15) Naphthalene 15.90 128 690921 15.93 ug/1 100 16) Hexachlorobutadiene 16.44 225 34597 5.04 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 5970 1.33 ug/1 96 19) 2-Chloronaphthalene 19.41 162 424559 15.85 ug/1 97 20) Dimethylphthalate 20.49 163 560739 18.16 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 120346 16.30 ug/1 95 22) Acenaphthylene 20.67 152 632060 16.86 ug/1 99 2 3) Acenaphthene 21.24 153 451951 16.96 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 151557 15.59 ug/1 99 25) Diethylphthalate 22.63 149 531835 17.95 ug/1 98 26) 4-Chlorophenyl-phenylether 22.78 204 237944 18.10 ug/1 99 27) Fluorene 22.76 166 504231 17.87 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 474950 15.15 ug/L 97 31) N-Nitrosodiphenyl amine 23.17 168 153611 12.31 ug/1 99 32) 4-Bromophenyl-phenylether 24.24 248 133801 18.37 ug/1 95 (#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Fri Apr 26 09:32:22 2002 Page 1

NYC-WTC_000049417