GCMS reference data for sample AE08839, April 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2302\REF2.D Vial: 5 Acq On : 23 Apr 2002 6:19 pm Operator: Sample : gc/ms scan 4/15 Inst : 209 Misc Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 8:10 2002 Quant Results File: GCMSO412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMSO412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMSO412

Internal Standards R.T. Qlon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) 1,4-Dichlorobenzene-d4 12.21 152 526883 20.00 ug/l -0.03 10) Naphthalene-d8 15.85 136 1914894 20.00 ug/l -0.03 17) Acenaphthene-d10 21.15 164 1098504 20.00 ug/l -0.03 30) Phenanthrene-d10 25.59 188 1608855 20.00 ug/l -0.03 39) Chrysene-d12 33.65 240 1098748 20.00 ug/l -0.03 45) Perylene-d12 37.87 . 264 703374 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 23.29 209 40517 7.36 ug/L -0.04 Spiked Amount 10.000 Recovery = 73.60% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 111322 9.71 ug/l 99 3) bis(2-Chloroethyl)ether 11.61 93 260043 14.57 ug/l 100 4) 1,3-Dichlorobenzene 12.11 146 169447 9.21 ug/l 99 5) 1,4-Dichlorobenzene 12.26 146 183605 9.91 ug/l 97 6) 1,2-Dichlorobenzene 12.77 146 193370 11.24 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.09 45 349110 14.16 ug/1 98 8) N-Nitroso-di-n-propylamine 13.47 70 163276 13.95 ug/l 99 9) Hexachloroethane 13.62 117 32191 4.74 ug/l 96 11) Nitrobenzene 13.89 77 233477 13.91 ug/l 99 12) Isophorone 14.54 82 372281 11.72 ug/l 99 13) bis(2-Chloroethoxy)methane 15.22 93 306870 14.83 ug/l 99 14) 1,2,4-Trichlorobenzene 15.73 180 172154 11.83 ug/1 99 15) Naphthalene 15.90 128 660147 14.34 ug/l 100 16) Hexachlorobutadiene 16.45 225 21797 2.99 ug/l 97 18) Hexachlorocyclopentadiene 18.64 237 4538 0.93 ug/l # 96 19) 2-Chloronaphthalene 19.40 162 416118 14.36 ug/1 99 20) Dimethylphthalate 20.50 163 523701 15.68 ug/l 99 21) 2,6-Dinitrotoluene 20.71 165 111099 13.91 ug/l 99 22) Acenaphthylene 20.68 152 606526 14.96 ug/l 100 23) Acenaphthene 21.24 153 430833 14.95 ug/l 99 24) 2,4-Dinitrotoluene 21.88 165 141953 13.50 ug/1 96 25) Diethylphthalate 22.62 149 501904 15.67 ug/l 100 26) 4-Chlorophenyl-phenylether 22.78 204 222235 15.63 ug/1 99 27) Fluorene 22.76 166 476004 15.60 ug/l 100 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 437790 12.91 ug/L 95 31) N-Nitrosodiphenylamine 23.17 168 151736 11.34 ug/1 100 32) 4-Bromophenyl-phenylether 24.25 248 125497 16.07 ug/l 94 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration REF2.D GCMSO412.M Wed Apr 24 08:13:44 2002 Page 1

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