GCMS calibration table for multiple compounds, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\l\DATA\APR1202\REF2.D Vial: 5 Acq On : 15 Apr 2002 12:00 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 15:00 2002 <Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 14:55:12 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.23 152 521869 20.00 ug/1 0.00 10) Naphthalene-d8 15.87 136 1943445 20.00 ug/1 0.00 17) Acenaphthene-diO 21.17 164 1100831 20.00 ug/1 0.00 30) Phenanthrene-diO 25.62 188 1615227 20.00 ug/1 0.00 39) Chrysene-dl2 33.67 240 1019420 20.00 ug/1 0.00 45) Perylene-dl2 37.91 264 661333 20.00 ug/1 0.00 System Monitoring Compounds 28) TCMX 23.31 209 39860 7.22 ug/L -0.02 Spiked Amount 10.000 Recovery = 72.20% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 102869 9.06 ug/1 96 3) bis(2-Chloroethyl)ether 11.62 93 251740 14.24 ug/1 100 4) 1,3-Dichlorobenzene 12.13 146 149088 8.18 ug/1 98 5) 1,4-Dichlorobenzene 12.28 146 163870 8.93 ug/1 99 6) 1,2-Dichlorobenzene 12.79 146 174921 10.27 ug/1 98 7) 2,2'-oxybis(1-Chloropropan 13.11 45 348444 14.27 ug/1 97 8) N-Nitroso-di-n-propylamine 13.50 70 167135 14.42 ug/1 99 9) Hexachloroethane 13.64 117 30193 4.49 ug/1 99 11) Nitrobenzene 13.91 77 224619 13.18 ug/1 99 12) 1sophorone 14.55 82 395659 12.27 ug/1 99 13) bis(2-Chloroethoxy)methane 15.24 93 302005 14.38 ug/1 99 14) 1,2,4-Trichlorobenzene 15.76 180 157278 10.65 ug/1 98 15) Naphthalene 15.92 128 638594 13.67 ug/1 100 16) Hexachlorobutadiene 16.47 225 22125 2.99 ug/1 97 18) Hexachlorocyclopentadiene 18.67 237 3953 0.81 ug/1 95 19) 2-Chloronaphthalene 19.43 162 396263 13.65 ug/1 99 20) Dimethylphthalate 20.51 163 555251 16.59 ug/1 98 21) 2,6-Dinitrotoluene 20.73 165 110459 13.80 ug/1 97 22) Acenaphthylene 20.70 152 611448 15.05 ug/1 99 23) Acenaphthene 21.26 153 433330 15.01 ug/1 99 24) 2,4-Dinitrotoluene 21.90 165 141030 13.39 ug/1 97 25) Diethylphthalate 22.65 149 538161 16.76 ug/1 99 26) 4-Chlorophenyl-phenylether 22.81 204 224810 15.78 ug/1 98 27) Fluorene 22.78 166 488549 15.98 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.27 77 456340 13.43 ug/L 99 31) N-Nitrosodiphenylamine 23.19 168 163649 12.18 ug/1 98 32) 4-Bromophenyl-phenylether 24.27 248 123762 15.78 ug/1 98 (#) = qualifier out of range (m) = manual integration REF2.D GCMS0412.M Tue Apr 16 15:01:56 2002 Page 1

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