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GCMS sample analysis report AE08435, Apr 18 2002

Machine-extracted title · confidence 95%

Gas chromatography-mass spectrometry results for sample AE08435 including surrogate recovery data.

NYC-WTC_000048561–000048570

Folder label: “GCMS X 4/10/02 A 4/15/02

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Scanned page image, NYC-WTC_000048566
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\l\DATA\APR1202\8435.D Vial: 24 Acq On : 16 Apr 2002 6:37 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.201 340 344 369 rBV 359050 901367 21.92% 4.193% 2 12.231 777 783 801 rBV 1092013 2766507 67.26% 12.869% 3 14.829 1060 1066 1073 rVB 328633 638342 15.52% 2.969% 4 15.867 1173 1179 1195 rBV 1667281 3578324 87.00% 16.645% 5 21.173 1750 1757 1773 rBV 1905381 4112957 100.00% 19.132% 6 23.303 1983 1989 1996 rBV 189346 395144 9.61% 1.838% 7 25.607 2233 2240 2252 rBV2 1786001 3947099 95.97% 18.361% 8 33.667 3111 3118 3137 rBV2 1239653 2866175 69.69% 13.332% 9 37.900 3571 3579 3601 rBV2 743548 2291816 55.72% 10.661%

Sum of corrected areas: 21497731 8435.D GCMS0412.M Wed Apr 17 09:48:11 2002

NYC-WTC_000048566

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NYC-WTC_000048566Source: NYC Law Department, mirrored locally

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