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GCMS analysis results, Sample AE08434, April 18, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08434 showing surrogate recovery and unknown compound screening on April 18, 2002.

NYC-WTC_000048550–000048560

Folder label: “GCMS X 4/10/02 A 4/15/02

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Scanned page image, NYC-WTC_000048555
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1202\8434.D Vial: 23 Acq On : 16 Apr 2002 5:38 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.379 140 145 161 rBV 36107 92248 2.37% 0.465% 2 8.205 340 344 370 rBV 286989 822372 21.17% 4.143% 3 12.226 777 782 798 rBV 1017840 2643276 68.03% 13.317% 4 14.824 1060 1065 1071 rBV 46055 93235 2.40% 0.470% 5 15.862 1172 1178 1195 rBV 1593155 3418315 87.98% 17.222%

6 21.168 1750 1756 1773 rBV 1920595 3885470 100.00% 19.575% 7 23.307 1981 1989 1996 rBV 201080 401386 10.33% 2.022% 8 25.611 2233 2240 2251 rBV 1773858 3710076 95.49% 18.692% 9 33.662 3110 3117 3137 rBV2 1135717 2682945 69.05% 13.517% 10 37.904 3570 3579 3599 rBV2 679764 2099595 54.04% 10.578%

Sum of corrected areas: 19848918

8434 .D GCMS0412.M Wed Apr 17 09:47:56 2002

NYC-WTC_000048555

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NYC-WTC_000048555Source: NYC Law Department, mirrored locally

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