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GCMS analysis results, Sample AE08432, April 18, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08432 showing surrogate recovery and unknown compound screening on April 18, 2002.

NYC-WTC_000048530–000048539

Folder label: “GCMS X 4/10/02 A 4/15/02

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Scanned page image, NYC-WTC_000048535
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1202\8432.D Vial: 21 Acq On : 16 Apr 2002 3:41 am Operator: Sample : gc/ms scan 4/10 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. . total

1 8.197 340 343 372 rBV 300128 801148 18.61% 3.806% 2 12.227 777 782 801 rBV 1166572 2898393 67.34% 13.769% 3 15.863 1172 1178 1194 rBV 1770853 3724380 86.53% 17.693% 4 21.169 1749 1756 1773 rBV 2087306 4304274 100.00% 20.448% 5 23.308 1982 1989 1995 rBV 211351 413497 9.61% 1.964%

6 25.612 2233 2240 2251 rBV 1878747 3978747 92.44% 18.902% 7 25.750 2251 2255 2270 rVB3 14527 56942 1.32% 0.271% 8 33.663 3110 3117 3136 rBV2 1158420 2788423 64.78% 13.247% 9 37.905 3570 3579 3600 rBV2 666296 2083946 48.42% 9.900%

Sum of corrected areas: 21049750

8432.D GCMS0412.M Wed Apr 17 09:47:27 2002

NYC-WTC_000048535

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NYC-WTC_000048535Source: NYC Law Department, mirrored locally

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