GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
NYC-WTC_000047979–000048003Folder label: “GCMS X 4/8/02 A 4/18/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\APRO102\5749.D Vial: 28 Acq On 3 Apr 2002 3:58 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 4:46 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorot>enzene-d4 12.25 152 499345 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1849633 20.00 ug/1 -0.11 17) Acenaphthene-diO 21.19 164 1033907 20.00 ug/1 -0.12 29) Phenanthrene-diO 25.64 188 1467581 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 733977 20.00 ug/1 -0.16 44) Perylene-dl2 37.93 264 398880 20.00 ug/1 -0.19
System Monitoring Compounds 37) 2,4-DDD 30.71 235 71934 4.89 ug/mL 0.21 Spiked Amount 5.000 Recovery = 97.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.93 128 417 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 1102 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 5749.D GCMS0403.M Fri Apr 05 10:32:52 2002 Page 1
NYC-WTC_000047981
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NYC-WTC_000048013
Gas chromatography-mass spectrometry analysis of sample AE08210 detecting unknown organic compounds and measuring 2,4-DDD surrogate recovery at 73%, April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048055
GCMS analysis report for sample AE08215 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048069
GCMS analysis report for sample AE08216 showing surrogate recovery and unknown compounds from April 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039545
Laboratory report documenting GCMS analysis of sample AE06452 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039522
Laboratory report documenting GCMS analysis of sample AE06450 conducted on April 19, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011877
Laboratory report documenting GCMS analysis of environmental sample AE04411 conducted on April 3, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058391
Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04592.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058325
Gas chromatography-mass spectrometry analysis of environmental sample AE04801 conducted April 4, 2002, detecting unknown compounds and surrogates.
Similar document embedding; no shared entity or topic indexed. · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000047951
Department of Environmental Protection GCMS analysis record dated April 8-18, 2002.
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NYC-WTC_000047952
Laboratory log sheet for Method 20 recording parameters and sample processing details from April 2002.
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GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
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GCMS calibration results for volatile organic compounds from sample AE08209 analyzed in April 2002.
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GCMS reference analysis report for volatile organic compounds from sample AE08209 analyzed in April 2002.
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