NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\APRO1O2\57O1.D Vial: 19
Acq On 2 Apr 2002 6:05 am Operator:
Sample gc/ms scan 3/12 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Apr 5 10:09 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Mar 29 10:31:28 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 579834 20.00 ug/1 -0.11
10) Naphthalene-d8 15.88 136 2137719 20.00 ug/1 -0.12
17) Acenaphthene-dlO 21.19 164 1209208 20.00 ug/1 -0.13
29) Phenanthrene-dlO 25.63 188 . 1712088m 20.00 ug/1 -0.14
38) Chrysene-dl2 33.69 240 849523 20.00 ug/1 -0.15
44) Perylene-dl2 37.94 264 483911 20.00 ug/1 -0.18
System Monitoring Compounds
37) 2,4-DDD 30.71 235 83106 4.84 ug/mL 0.21
Spiked Amount 5.000 Recovery = 96.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 14 6 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.95 128 290 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluehe 0.00 165 0 N.D.
25) Diethylphthalate 22.67 149 1289 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
5701.D GCMS0403.M Fri Apr 05 10:09:56 2002 Page 1
NYC-WTC_000059501
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