NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\APR0102\5696.D Vial: 11
Acq On 1 Apr 2002 10:10 pm Operator :
Sample gc/ms scan 3/11 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Apr 1 22:59 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Mar 29 10:31:28 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Mih)
1) 1,4-Dichlorobenzene-d4 12.25 152 524053 20.00 ug/1 -0.11
10) Naphthalene-d8 15.88 136 1922486 20.00 ug/1 -0.12
17) Acenaphthene-dlO 21.19 164 1073723 20.00. ug/1 -0.12
29) Phenanthrene-dlO 25.63 188 1489667 20.00 ug/1 -0.13
38) Chrysene-dl2 33.69 240 732296 20.00 ug/1 -0.15
44) Perylene-dl2 37.93 264 408026 20.00 ug/1 -0.19
System Monitoring Compounds
37) 2,4-DDD 30.71 235 75827 5.07 ug/mL 0.21
Spiked Amount 5.000 Recovery = 101^40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene ■ 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 0.00 128 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0. N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2., 4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.68 149 772 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
5696.D GCMS0403.M Thu Apr 04 12:57:38 2002 . Page 1
NYC-WTC_000059260
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