GCMS blank analysis, sample AE05515, April 2002

Machine-extracted title · confidence 100%

Blank quality control GCMS analysis of sample AE05515 conducted April 4, 2002, showing below-detection-limit results for sixteen organic compounds.

NYC-WTC_000059210–000059217

Folder label: “GCMS X 3/11/02 A 4/1/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO10 2\LB.D Vial: 3 Acq On 1 Apr 2002 1:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 14:00 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 587663 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 2160949 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 1216459 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.64 188 1704799 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 240 875057 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 480015 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 235 88631 5.18 ug/mL 0.21 Spiked Amount 5.000 Recovery = 103.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.94 128 239 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.68 149 1163 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration LB.D GCMS0403.M Thu Apr 04 12:12:17 2002 Page 1

NYC-WTC_000059211

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000059211Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GC/MS blank analysis results, April 17 2002 · Box DEP Box 57

NYC-WTC_000060438

Laboratory report showing GC/MS blank analysis for Method 508 compounds with non-detectable levels.

1 shared topics · Same agency, volume and box · similarity 0.997