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GCMS unknown compound analysis, sample AE05696, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.

NYC-WTC_000059258–000059266

Folder label: “GCMS X 3/11/02 A 4/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) '

Data File C:\HPCHEM\1\DATA\APRO1O2\5696.D ■ Vial: 11 Acq On 1 Apr 2002 10:10 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 22:59 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri' Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.64 178 462 N.D. 34) Anthracene 25.64 178 462 N.D. 35) Di-n-butylphthalate 27.61 149 18158 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.69 228 1561 N.D. 42) Bis(2-ethylhexyl)phthalate 33.90 149 1677 N.D. 43) Chrysene 33.69 228 1561 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.76 252 102 N.D. 47) Benzo(k)fluoranthene 36.83 252 271 N.D. 48) Benzo(a)pyrene 37.94 252 1438 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 5696.D GCMS0403.M Thu Apr 04 12:57:42 2002 Page 2

NYC-WTC_000059261

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NYC-WTC_000059261Source: NYC Law Department, mirrored locally

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