NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\APR0102\5748.D Vial: 27
Acq On 3 Apr 200.2 2:58 am Operator:
Sample gc/ms scan 3/12 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Apr 3 3:47 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Mar 29 10:31:28 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 513161 20.00 ug/1 . -0.10
10) Naphthalene-d8 15.89 136 1924743 20.00 ug/1 -0.11
17) Acenaphthene-dlO 21.19 164 1080639 20.00 ug/1 -0.12
29) Phenanthrene-dlO 25.64 188 1504965 20.00 ug/1 -0.13
38) Chrysene-dl2 33.69 240 753707 20.00 ug/1 -0.16
44) Perylene-dl2 37.93 264 404523 20.00 ug/1 -0.19
System Monitoring Compounds
37) 2,4-DDD 30.70 235 78818 5.22 ug/mL 0.21
Spiked Amount 5.000 Recovery = 104.40%
- Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.56 74 185 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 ' 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-bxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.93 128 360 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.67 149 1082 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
{#) = qualifier out of range (m) = manual integration
5748.D GCMS0403.M Fri Apr 05 10:28:51 2002 Page 1
NYC-WTC_000059578
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