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GCMS analysis results for sample AE05747, April 11 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05747 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059576–000059584

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APRO102\5748.D Vial: 27 Acq On 3 Apr 2002 2:58 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 3 3:47 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.64 178 409 N.D. 34) Anthracene 25.64 178 409 N.D. 35) Di-n-butylphthalate 27.60 149 10007 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.69 228 1711 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 1357 N.D. 43) Chrysene 33.69 228 1711 N.D. 45) Di-n-Octylphthalate 35.68 149 171 N.D. 46) Benzo(b)fluoranthene 36.74 252 44 0 N.D. 47) Benzo(k)fluoranthene 36.85 252 645 N.D. 48) Benzo(a)pyrene 37.74 252 338 N'.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0. N.D.

(#) = qualifier out of range (m) = manual integration 5748.D GCMS0403.M Fri Apr 05 10:28:55 2002 Page 2

NYC-WTC_000059579

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NYC-WTC_000059579Source: NYC Law Department, mirrored locally

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