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GCMS analysis results for sample AE05702, April 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05702 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059517–000059525

Folder label: “GCMS X 3/12/02 A 4/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0102\5703.D Vial: 21 Acq On 2 Apr 2002 8:04 am Operator: Sample gc/ms scan 3/12 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 8:53 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.63 178 616 N.D. 34) Anthracene 25.63 178 616 N.D. 35) Di-n-butylphthalate 27.60 149 21362 0.26 ug/1 99 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.69 228 1632 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 5210 N.D. 43) Chrysene 33.76 228 209 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.94 252 1628 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 5703.D GCMS0403.M Fri Apr 05 10:14:28 2002 Page 2

NYC-WTC_000059520

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NYC-WTC_000059520Source: NYC Law Department, mirrored locally

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