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GCMS unknown compound analysis, sample AE05516, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.

NYC-WTC_000059286–000059295

Folder label: “GCMS X 3/11/02 A 4/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\APR0102\5516.D Vial: 7 f Acq On 1 Apr 2002 6:11 pm Operator: /Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS integration Params: GOOFY.P Quant Time: Apr 1 19:00 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.64 178 541 N.D. 34) Anthracene 25.64 178 541 ■' N.D. 35) Di-n-butylphthalate 27.60 149 7234 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 . n.d: 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.70 228 2144 N.D. 42) Bis(2-ethylhexyl)phthalate 33.90 149 1538 N.D. 43) Chrysene 33.76 228 428 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 36.76 252 480 N.D. 47) Benzo(k)fluoranthene 36.84 252 652 N.D. 48) Benzo(a)pyrene 37.94 252 1933 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (tn) = manual integration 5516.D GCMS0403.M Thu Apr 04 12:46:50 2002 Page 2

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NYC-WTC_000059289Source: NYC Law Department, mirrored locally

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