GCMS analysis results for sample AE08252, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On 17 Apr 2002 4:52 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

37.92 0.34 ug/L 335278 Perylene-dl2 34.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5 -hexamet... 384 C12H3604Si5 003555-47-3 10 2 Propanoic acid, 2- [(trimethylsil . . . 234 C9H2203Si2 017596-96-2 9 3 2-Pentenoic acid, 2-[(trimethyls... 260 CllH24O3Si2 055045-17-5 9 4 Propanoic acid, 2-[(trimethylsil ... 234 C9H2203Si2 017596-96-2 9 Abundance Scan 5930 (37.921 min): 08252.D (-5914) (-) m/z 73.05 100.00% 73 147 221

5000 355 281 429 40 37 60 37 80 38.00 38 20 01 I I | 191 1 .1 m/z 147.00 97.90% n/z- > 50 100 150 200 250 300 350 400 Abundance #26961 Trisiloxane, 1,1,1,5,5,5-hexamethy-3,3-bis[(trime . 73 147 281 5000 ■ 1 ...... ■ । ■ ■ ' 1 i 37 60 37 80 38.00 38.20

369 m/z 221.00 67.92% 27 45 207 20 01 - TIr 95 117 +,177.4.226.249,1 , 310,341, J- Ti/Z--> 50 100 150 200 250 300 350 400 Abundance #123316: Propanoic acid, 2-[(trimethylsilyl)oxy]-, trimeth.. 73 117 147

37.60 37 80 38 00 38 20 5000 m/z 355.00 39.95%

191 A

01 55 ।' 99 ■A , 150 1 50 t ' 100 t 173 J — r । 'i 219 'i i i — V n/z- > Abundance 200 250 #115080: 2-Pentenoic acid, 2-[(trimethylsilyl)oxy]-, trime. . 300 350 400 ....... ill........ , 73 147 37 60 37.80 38.00 38 20 m/z 281.00 29.90%

5000 45 1 0 113 L II .172 201 245 .3........ Aylls MaMsbt Tl/Z-> 100 150 200 250 300 350 400 37.60 37 80 38 00 38.20

08252.D 041702SCAN.M Thu Apr 18 09:14:05 2002 Page 23

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