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GCMS analysis results for sample AE08252, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.

NYC-WTC_000047802–000047829

Folder label: “GCMS X 4/8/02 A 4/17/02

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Scanned page image, NYC-WTC_000047825
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08252.D Vial: 10 Acq On : 17 Apr 2002 4 : 52 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 15 IH-Indene, 2-butyl-3-hexyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

34.96 0.30 ug/L 289116 Perylene-dl2 34.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 IH-Indene, 2-butyl-3-hexyl- 256 C19H28 054986-54-8 25 2 1-Hydroxymethyl-1,2,3,4-tetrahyd... 178 C11H1402 1000187-34-9 23 3 3 -(3,4-Dimethyl-6-Phenylcyclohex.. . 256 C17H20O2 1000215-26-9 9 4 2-Chloro-4-aminopyrimidine 129 C4H4C1N3 007461-50-9 9 Abundance Scan 5427 ( 34 966 min): 08252.D (-5425) (-) m/z 40.00 100.00% 43 129

5000 281 73 86 258 116 I 207

n/z-> 0+ i ’ ' :20 - 40 60 LI. 7. 80 100 120 140 160 180 200 220 ■ i ■ • ' ■ i ‘ ■ i ■ ' 1 ■ i ■ ■ ■ ■ i ' ‘ 240 ii i ' 1 ■ ' l ' 1 260 280 34 60 34.80 35 00 35 20 m/z 129.60 67.67% Abundance #58459 1H-lndene, 2-butyl-3-hexyl- 1 9 143 41 5000 ‘I U‘ ■ ' I 115 213 256 34 60 34 80 35 00 35 20 55 m/z 130.20 44.50% 91 1551 171 185 199 69

n/z-> 01 1′114 20 40 60 11 A 4193. 80 100 120 140 160 180 200 220 240 4. , 11 227 243 , 260 280 Abundance #58457: 1-Hydroxymethyl-1,2,3.4-tetrahydro-naphthalen-2-ol 1 79

34.60 34 80 35.00 35 20 5000 117 m/z 281.00 44.33% 91 160 105 142 , 77 97 39 51 63 I 0 -- Tr F— ' 1 i ' ' 1 ' i 1 ' 1 ' i ■ ' ■ ' i ■ 1 ' ' i ' 1 ' 1 i n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58556 3-(3.4-Dimethyl-6-Phenylcyclohex-3-enyl)prop-2-eno . 119 34.60 34 80 35.00 35.20 m/ Z 86.00 35.33% 5000 174 91 256 41 65ii 77 /z- > |L. 53 0 I 1 ' ' 1 r' ' 1 1 I 1 ' ' 'I,.r ■ ' 20 40 M.

60 80 ,193116 100 120 140 160 180 | 197 214 200 220 239 240 260 280 n/ana AM । । My***MMr, । M 34 60 34.80 35 00 35 20

08252 .D 041702SCAN.M Thu Apr 18 09:14:04 2002 Page 2 0

NYC-WTC_000047825

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NYC-WTC_000047825Source: NYC Law Department, mirrored locally

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