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GCMS reference analysis results for sample AE08012, April 2002

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Laboratory report of GCMS reference analysis for sample AE08012 conducted on April 17, 2002, showing recovery percentages for target compounds.

NYC-WTC_000047656–000047663

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1102\REFA2.D Vial: 17 Acq On : 12 Apr 2002 6:07 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 11:51 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:47:07 2002 Response via : Initial Calibration DataAcq Meth : GCMS0408

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.70 284 150172 19.61 ug/1 99 34) Phenanthrene 25.68 178 674699 19.59 ug/1 99 35) Anthracene 25.80 178 604788 17.86 ug/1 100 36) Di-n-butylphthalate 27.58 149 977609 22.69 ug/1 99 37) Fluoranthene 29.29 202 657327 18.98 ug/1 100 .40) Pyrene 29.97 202 679023 20.71 ug/1 100 41) Butylbenzylphthalate 32.10 149 317742 19.81 ug/1 100 42) Benzo(a)anthracene 33.61 228 442012 19.43 ug/1 98 43) Bis(2-ethylhexyl)phthalate 33.88 149 425877 20.76 ug/1 98 44) Chrysene 33.74 228 468726 20.78 ug/1 99 46) Di-n-Octylphthalate 35.62 149 542160 17.92 ug/1 # 98 47) Benzo(b)fluoranthene 36.71 252 357328 18.28 ug/1 98 48) Benzo(k)fluoranthene 36.78 252 400232 21.03 ug/1 98 4 9) Benzo(a)pyrene 37.70 252 247985 15.39 ug/1 99 50) Indeno(1,2,3-cd)pyrene 41.99 276 277509 17.10 ug/1 100 51) Dibenz(a,h)anthracene 42.06 278 238773 19.30 ug/1 99 52) Benzo(g,h,i)perylene 43.23 276 255789 18.88 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Tue Apr 16 11:53:26 2002 Page 2

NYC-WTC_000047662

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NYC-WTC_000047662Source: NYC Law Department, mirrored locally

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