GCMS reference analysis results for sample AE08012, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1102\REFA2.D Vial: 17 Acq On : 12 Apr 2002 6:07 am Operator : Sample : gc/ms scan 4/4 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 11:51 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:47:07 2002 Response via : Initial Calibration DataAcq Meth : GCMS0408

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.23 152 447938 20.00 ug/1 -0.01 10) Naphthalene-d8 15.86 136 1648215 20.00 ug/1 -0.01 17) Acenaphthene-diO 21.17 164 925046 20.00 ug/1 0.00 30) Phenanthrene-diO 25.61 188 1333342 20.00 ug/1 0.00 39) Chrysene-dl2 33.66 240 816232 20.00 ug/1 -0.01 45) Perylene-dl2 37.90 264 512125 20.00 ug/1 -0.02

System Monitoring Compounds 2 8) TCMX 23.31 209 38554 7.75 ug/L -0.02 Spiked Amount 10.000 Recovery = 77.50% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 110620 11.35 ug/1 99 3) bis(2-Chloroethyl)ether 11.62 93 255918 16.87 ug/1 99 4) 1,3-Dichlorobenzene 12.13 146 207444 13.26 ug/1 99 5) 1,4-Dichlorobenzene 12.27 146 219397 13.93 ug/1 98 6) 1,2-Dichlorobenzene 12.79 146 213945 14.63 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.11 45 368823 17.59 ug/1 100 8) N-Nitroso-di-n-propylamine 13.49 70 171537 17.24 ug/1 97 9) Hexachloroethane 13.64 117 61462 10.65 ug/1 96 11) Nitrobenzene 13.91 77 231661 16.03 ug/1 98 12) Isophorone 14.56 82 442917 16.20 ug/1 100 13) bis(2-Chloroethoxy)methane 15.24 93 308659 17.33 ug/1 99 14) 1,2,4-Trichlorobenzene 15.75 180 184482 14.72 ug/1 99 15) Naphthalene 15.92 128 669148 16.89 ug/1 99 16) Hexachlorobutadiene 16.47 225 69459 11.08 ug/1 98 18) Hexachlorocyclopentadiene 18.66 237 7410 1.81 ug/1 # 91 19) 2-Chloronaphthalene 19.42 162 401503 16.46 ug/1 99 20) Dimethylphthalate 20.52 163 544964 19.38 ug/1 99 21) 2,6-Dinitrotoluene 20.73 165 110705 16.46 ug/1 99 22) Acenaphthylene 20.70 152 623224 18.26 ug/1 99 23) Acenaphthene 21.26 153 443135 18.26 ug/1 99 24) 2,4-Dinitrotoluene 21.89 165 140751 15.90 ug/1 97 25) Diethylphthalate 22.65 149 533982 19.79 ug/1 100 26) 4-Chlorophenyl-phenylether 22.80 204 224033 18.72 ug/1 100 27) Fluorene 22.78 166 489615 19.06 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.26 77 480278 16.82 ug/L 99 31) N-Nitrosodiphenylamine 23.19 168 138866 12.52 ug/1 99 32) 4-Bromophenyl-phenylether 24.27 248 123233 19.04 ug/1 95

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Tue Apr 16 11:53:25 2002 Page 1

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