GCMS calibration results for sample AE07972, April 2002

2 z Quantitation Report (QT Reviewed) K K o s o

o Data File Acq On : C:\MSDCHEM\l\DATA\020415\0415C3.D : 15 Apr 2002 11:25 am Vial : 2 Operator: Nefliu co — "0 I Sample : ccv Inst : Instrumen C o O o Miso : o Multiplr: 1.00 o' o MS Integration Params: EVENTS.E “O o C Quant Time: Apr 16 11:02 2002 Quant Results File: 041202SCAN.RES — N 0 O Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) o Q C Title : 508 Modified GC/MS scan 3 Last Update : Tue Apr 16 11:02:14 2002 CD 3 Response via : Initial Calibration Abundance TIC: 0415C3.D 9000000

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Time—> 0 PM— । । 4.00 6 00 ‘ ' 1 1 8.00 10.00 12 00 r PI ■ 14.00 16.00 18 00 4 — — Tr f - 24 00 20.00 26 00 J — r pl-pi 22.00 28 00 30 00 — 32.00 34.00 36 oo 38 00

0415C3.D 041202SCAN.M Tue Apr 16 11:03:03 2002 Page 3