GCMS analysis results, sample AE07517, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07517.D Vial: 13 Acq On 4 Apr 2002 6:09 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Bis(2-ethylhexyl) maleate Concentration Rank I

R.T. EstConc Area Relative to ISTD R.T.

36.17 3.60 ug/1 3848330 Chrysene-dl2 39.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Bis(2-ethylhexyl) maleate 340 C20H36O4 000142-16-5 62 2 1,2-Cyclohexanedione 112 C6H802 000765-87-7 43 3 Diisooctyl maleate 340 C20H36O4 001330-76-3 40 4 3-Piperidinone, 1-acetyl-6-methyl- 155 C8H13NO2 054751-97-2 35 Abundance Scan 5632 (36.171 min): 07517.D (-5601) (-) m/z 57.10 100.00% 57

100117 5000 4* 83 ' I ' 1 ■ ' I ' 211 35.80 36.00 36 20 36.40 36.60 0- 185 . 229 — :WWT11UIITETTTHT)***1C*ITTITITTTTTTT m/z 70.10 '' I' • 99.48% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #17609: Bis(2-ethylhexyl) maleate 57 1 7

41 5000 100 35.80 36.00 36.20 36.40 36.60 83 m/z 71.10 65.08%

m/z-> 0- .5.41. ,■ , 4 , , 4 ! 41 I I' 139 297 169185 341 212229 1 ■ I ■ ■1 ■ i ri’ ' 1*1 ' i'11 > i • 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■i

Abundance #120179:1,2-Cyclohexanedione 1* 2 "htt ■ - I I I IT 35.80 36.00 36.20 36.40 36.60 5000 70 m/z 100.00 59.34% 43

/z-> o1 T-q-r 20 XL | 94 ' I " " I " '' I " " I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #52271: Diisooctyl maleate 57 1* 7 35.80 36.00 36.20 36.40 36.60 m/z 117.00 55.80% 100 41 5000 83

n/z—> 0 lLl T . . 141 167 185 . 211 229_____ 283 311 340 ‘11 1 'I T*' I" 1 '1'' I hi. I.... 1.... 1.... 1 7 111111111 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ‘ I 1 1 ' ' I 35.80 36.00 36.20 36.40 36.60 V

NYC-WTC_000047426