GCMS analysis results, sample AE07513, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020404\07513.D Vial: 9 Acq On 4 Apr 2002 2:26 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Acetonitrile, dichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 3.31 0.18 ug/1 114691 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 28 2 Thiirane, methyl- 74 C3H6S 001072-43-1 4 3 N-Nitrosodimethylamine 74 C2H6N20 000062-75-9 2 4 Hydrazinecarboximidamide 74 CH6N4 000079-17-4 2 Abundance Scan 39 (3.308 min): 07513.D (-35) (-) m/z 74.00 100.00% 74 40 82 5000 .............................................................. I 1 1 1 1 , ' 'll I 47 3.20 3.30 3.40 3.50 3.60 3.70 01 ' i' ■11111111' r '1' i' i ■ ■ ■ ■ i • ■ • ■ i m/z 40.10 XA~-V- 59.00% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 TI[rTTrTEI1t1‘rTI1‘—Wh3"‘IITTUIT 3.20 3.30 3.40 3.50 3.60 3.70 38 47 m/z81.90 53.95%

m/z—> 01 —PO— 15 20 25 30 35 40 45 50 55 T TPPT I < ■■ ■ i ■ 86 TPT 60 65 70 75 80 85 90 95 Abundance #115343: Thiirane, methyl- 4.1 74 ' 1 1 I 1 ' ‘ ' 1 1 1 • ' I ‘ ' I ' I I I | VI I I | i I I I | 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 84.00 26.86% 45

QC > 27 30 33 n/Myyuop m/z-> 0 -152+ +8,53,5659.64.6871177. I I I I 11 j l 11

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 '11'' ■11' ■ ■ ■ i

Abundance #115351: N-Nitrosodimethylamine ‘ ‘I‘‘‘‘A‘‘‘‘I‘‘‘+A‘TIIIIEIIIS‘‘I] 74 3.20 3.30 3.40 3.50 3.60 3.70 42 m/z 47.00 23.30% 5000 28 J m/z—> 0 —TTH +31. —39 fR. 59 10901112213—171 I ■ ■ ■ ■ ।1111111111111' i ■' i " "i11 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.30 3.40 3.50 3.60 3.70

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