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GCMS reference standard results for volatile organics, April 2002

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Reference standard analysis report for GCMS testing of volatile organic compounds conducted on April 2-3, 2002.

NYC-WTC_000047186–000047188

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020403\0402REF2.D Vial: 12 Acq On 3 Apr 2002 7:13 pm Operator: Nefliu Sample 04/02 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 04 08:41:07 2002 Quant Results File: SCAN020403.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Thu Apr 04 08:40:00 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

37) Fluoranthene 35.23 202 4671235 8.54 ug/1 98 40) Pyrene 35.83 202 4950594 9.35 ug/1 99 41) Buthylbenzylphthalate 38.10 149 1403956 7.23 ug/1 100 42) Benz(a)anthracene 39.08 228 4152521 8.96 ug/1 99 43) Chrysene 39.16 228 4236760 9.78 ug/1 100 44) Bis(2-ethylhexyl)phthalate 39.68 149 1681462 6.82 ug/1 97 46) Di-n-Octyl phthalate 41.19 149 1874522 6.66 ug/1 98 47) Benzo(b)fluoranthene 41.53 252 3341777 9.22 ug/1 98 48) Benzo(k)fluoranthene 41.59 252 3593591 9.12 ug/1 97 4 9) Benzo(a)pyrene 42.17 252 2178911 6.56 ug/1 98 50) Indeno(1,2,3-cd)pyrene 44.35 276 1480255 8.47 ug/1 97 51) Dibenz(a,h)anthracene 44.45 278 1883651 7.45 ug/1 97 52) Benzo(ghi)perylene 44.89 276 1939390 .7.10 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0402REF2.D SCANO20403 . M Thu Apr 04 08:41:49 2002 Page 2

NYC-WTC_000047187

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NYC-WTC_000047187Source: NYC Law Department, mirrored locally

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