GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Ethanone, 1-cyclopropyl-, o.. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 30.07 0.37 ug/L 374587 Chrysene-dl2 30.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanone, 1-cyclopropyl-, oxime 99 C5H9NO 1000221-89-7 9 2 2-Methyl-3-vinyl-oxirane 84 C5H80 006790-37-0 3 3 2-Octenoic acid 142 C8H14O2 001470-50-4 2 4 Furo[3,4-b]furan-2,6 (3H,4H)-dion... 266 C15H2204 020223-76-1 2 Abundance Scan 4593 (30 066 min) 07766 D (-4587) (-) m/z 40.20 100.00% 4b

5000 243 83 109 56 67 99 29.80 30.00 3020 30.40 0- 1 1 1 1 ’ ' ■ ' 1 m/z 243.40 39.84% /z- > 20 40 60 80 100 120 140 160 180 200 220 240 A Abundance #1242: Ethanone, 1-cyclopropyl-, oxime 39

82 5000- 55 98 ■ > । ■ > > ■ । ■ ‘ I‘* 27 67 29.80 30.00 30.20 30.40 m/z 83.30 39.03%

m/z-> 01

Abundance 20 40 100 120 140 160 180 200 220 240 UWWAAWBWWwHop #1297 2-Methyl-3-vinyl-oxirane 39 55

' ' '29'80' 30'00' '30'20 30.40 5000- 83 m/z 82.30 33.37% 27 69

0 —1 Tl/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #108054: 2-Octenoic acid 29 41 29 80 30.00 30.20 30.40 m/z 244.30 32.56% 55 73 5000

86 9g 113 124 142........ O-t-j-r MJ 11 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 29.80 30.00 30'20' 30Vo'

07766.D 041202SCAN.M Tue Apr 16 13:42:11 2002 Page 14

NYC-WTC_000046882