GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 12 1,2,5-Oxadiazole Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

30.55 0.37 ug/L 372928 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,2,5-Oxadiazole 70 C2H2N20 000288-37-9 4 2 Thiocyanic acid, 2-propynyl ester 97 C4H3NS 024309-48-6 3 3 2-(1-Cyclohexenyl)ethylamine 125 C8H15N 003399-73-3 3 4 2-Pentanol, 5-(2-propynyloxy)- 142 C8H14O2 055702-67-5 2 Abundance Scan 4675 (30 548 min): 07766.D (-4666) (-) m/z 40.20 100.00% 4b

5000 70 57 85 97 125 1 1 I 1 '

111 30.20 30.40 30.60 30.80 000 ! | | I | , , 1 1, 1"0 1 i ' ■ m/z 70.40 40.52% n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1414: 1,2,5-Oxadiazole 4b

5000- 70 30.20 30.40 30.60 30.80

A 28 m/ z 85.30 35.93% 0t I | I I T I | 1 I 1 I | I 1

ti/z—>______ 0 10 20 I 30 —4 4050 60 1 i 1 ' 1 ■ i 1 70 80 90 100 110 120 130 Abundance #1364: Thiocyanic acid, 2-propynyl ester 39 97 30.20 30.40 30.60 30.80 5000 70 m/z 57.30 34.10%

4 12 2 32 26 I , 0^ I I I > I I I I I' I I I I I I’l’i I ll I 45

L511644— , 58 ■ i ■ ■ ■ ■ i ■ nil’ > > । > । । । । i । । । ■ ylwo"lpA n/z- > 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #877 2-( 1-Cyclohexenyl)ethylamine 33 30.20 30.40 30.60 30.80 m/z97.30 26.91%

5000

18 41 55 67 81 96 108 125 0 -PmP-mmmm Tl/Z— > 0 10 20 30 40 50 60 70 80 90 100 110 120 130 30.20 30.40 30.60 30.80

07766.D 041202SCAN.M Tue Apr 16 13:42:12 2002 Page 15

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