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GCMS results for sample AE08068, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08068 including surrogate recovery and unknown compounds on April 18, 2002.

NYC-WTC_000046813–000046840

Folder label: “GCMS X 4/5/02 A 4/16/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 16 13:56:14 2002. Quant Results File: 041202SCAN. RE

Quant Method C:\MSDCHEM\l\METHQDS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Last Update Tue Apr 16 11:14:47 2002 Response via Initial Calibration DataAcq Meth 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.99 152 4571083 40.00 ug/L 0.00 10) Napthalene-d8 13.48 136 17258161 40.00 ug/L -0.02 17) Acenapthalene-dlO 18.63 164 10011692 40.00 ug/L -0.01 29) Phenanthranene-dlO 23.02 188 15343823 40.00 ug/L -0.01 37) Chrysene-dl2 30.88 240 12116549 40.00 ug/L -0.03 43) Perylene-dl2 34.78 264 7878891 40.00 ug/L -0.02

System Monitoring Compounds 2 7) TCMX 20.60 207 337821 6.09 ug/L 0.00 Spiked Amount 8,000 Recovery = 76.13%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed 08068.D 041202SCAN.M Tue Apr 16 13:56:33 2002 Page 1

NYC-WTC_000046815

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NYC-WTC_000046815Source: NYC Law Department, mirrored locally

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